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aluminum dust 33% ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ sodium nitrate 65% magnesium dust 30% ? unpredictable
sulfur 5% burn rate ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium permanganate 60% glycerine 40% 4 delay before
ignition depends
upon grain size WARNING: IGNITES SPONTANEOUSLY WITH GLYCERINE!!! ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium permanganate 67% sulfur 33% 5 unstable ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium permangenate 60% sulfur 20% 5 unstable
magnesium or
aluminum dust 20% ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium permanganate 50% sugar 50% 3 ? ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium nitrate 75% charcoal 15% 7 this is
sulfur 10% black powder! ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium nitrate 60% powdered iron 1 burns very
or magnesium 40% hot ============================================================== potassium chlorate 75% phosphorus 8 used to make
sesquisulfide 25% strike
anywhere matches ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ammonium perchlorate 70% aluminum dust 30% 6 solid fuel
and small amount of for space
iron oxide shuttle ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium perchlorate 67% magnesium or 10 flash powder (sodium perchlorate) aluminum dust 33% ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium perchlorate 60% sulfur 20% or 8 alternate (sodium perchlorate) magnesium flash powder
aluminum dust 20% ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ barium nitrate 30% aluminum dust 30% 9 alternate potassium perchlorate 30% flash powder ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ barium peroxide 90% magnesium dust 5% 10 alternate
aluminum dust 5% flash powder ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium perchlorate 50% sulfur 25% 8 slightly
magnesium or unstable
aluminum dust 25% ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium chlorate 67% red phosphorus 27% 7 very unstable calcium carbonate 3% sulfur 3% impact sensitive ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium permanganate 50% powdered sugar 25% 7 unstable;
aluminum or ignites if
magnesium dust 25% it gets wet! ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ potassium chlorate 75% charcoal dust 15% 6 unstable
sulfur 10% ============================================================== NOTE: Mixtures that use substitutions of sodium perchlorate for potassium perchlorate become moisture-absorbent and less stable.
The higher the speed number, the faster the fuel-oxodizer mixture burns AFTER ignition. Also, as a rule, the finer the powder, the faster the rate of burning.
As one can easily see, there is a wide variety of fueloxodizer mixtures that can be made at home. By altering the amounts of fuel and oxodizer(s), different burn rates can be achieved, but this also can change the sensitivity of the mixture.
3.24 PERCHLORATES
As a rule, any oxidizable material that is treated with perchloric acid will become a low order explosive. Metals, however, such as potassium or sodium, become excellent bases for flash-type powders. Some materials that can be perchlorated are cotton, paper, and sawdust. To produce potassium or sodium perchlorate, simply acquire the hydroxide of that metal, e.g. sodium or potassium hydroxide. It is a good idea to test the material to be perchlorated with a very small amount of acid, since some of the materials tend to react explosively when contacted by the acid. Solutions of sodium or potassium hydroxide are ideal.
3.3 HIGH-ORDER EXPLOSIVES
High order explosives can be made in the home without too much difficulty. The main problem is acquiring the nitric acid to produce the high explosive. Most high explosives detonate because their molecular structure is made up of some fuel and usually three or more NO2 ( nitrogen dioxide ) molecules. T.N.T., or Tri-Nitro-Toluene is an excellent example of such a material. When a shock wave passes through an molecule of T.N.T., the nitrogen dioxide bond is broken, and the oxygen combines with the fuel, all in a matter of microseconds. This accounts for the great power of nitrogenbased explosives. Remembering that these procedures are NEVER TO BE CARRIED OUT, several methods of manufacturing high-order explosives in the home are listed.
3.31 R.D.X.
R.D.X., also called cyclonite, or composition C-1 (when mixed with plasticisers) is one of the most valuable of all military explosives. This is because it has more than 150% of the power of T.N.T., and is much easier to detonate. It should not be used alone, since it can be set off by a not-too severe shock. It is less sensitive than mercury fulminate, or nitroglycerine, but it is still too sensitive to be used alone. R.D.X. can be made by the surprisingly simple method outlined hereafter. It is much easier to make in the home than all other high explosives, with the possible exception of ammonium nitrate.
MATERIALS EQUIPMENT ~~~~~~~~~ ~~~~~~~~~ hexamine 500 ml beaker
or glass stirring rod methenamine funnel and filter paper fuel tablets (50 g) ice bath container concentrated (plastic bucket) nitric acid (550 ml) centigrade thermometer distilled water blue litmus paper table salt ice ammonium nitrate
1) Place the beaker in the ice bath, (see section 3.13, steps 3-4) and carefully pour 550 ml of concentrated nitric acid into the beaker.
2) When the acid has cooled to below 20 degrees centigrade, add small amounts of the crushed fuel tablets to the beaker. The temperature will rise, and it must be kept below 30 degrees centigrade, or dire consequences could result. Stir the mixture.
3) Drop the temperature below zero degrees centigrade, either by adding more ice and salt to the old ice bath, or by creating a new ice bath. Or, ammonium nitrate could be added to the old ice bath, since it becomes cold when it is put in water. Continue stirring the mixture, keeping the temperature below zero degrees centigrade for at least twenty minutes.
4) Pour the mixture into a litre of crushed ice. Shake and stir the mixture, and allow it to melt. Once it has melted, filter out the crystals, and dispose of the corrosive liquid.